스테파노 Stefano   14-06-05 17:41 (1) Pressure-Swing-Distillation은 혼합물이 공비점을 가지고 있어서 단순증류로 분리되지 않는 경우에 적용하는 방법의 하나입니다.  압력을 달리하면 공비점이 없어지는 경우라면 단순히 압력만 달리하면 되지만 압력이 달라짐에 따라 공비점 농도가 달라지는 경우에 사용되는 방법입니다.  이곳을 먼저 찾아보도록 하세요. http://en.wikipedia.org/wiki/Azeotrope#Pressure_swing_distillation http://www.separationprocesses.com/Distillation/DT_Chp06g.htm (2) 논문이 잘못된 것이 아닙니다.  언급한 논문을 자세히 읽어보면 왜 두번째 탑하부로 비점낮은 물질이 얻어지는지 알 수 있을 것입니다.  질문의 경우, 위의 두번째 URL링크에 소개된 경우와 같은 조건에서 운전되는 것입니다. (공비혼합물이 각 물질의 비점보다 낮은 비점을 가지고 압력을 높이면 공비점이 높은 농도쪽으로 이동하는 경우에 해당합니다.) (3) 분리원리 첫번째 탑은 저압으로 운전되는데 일반 증류탑에서와 같이 고비점 물질의 비점이 혼합물의 비점보다 더 높으므로 탑의 하부로 순수한 (상압에서의) 고비점 물질이 얻어집니다.  상부로는 낮은 비점의 고비점/저비점이 혼합물 상태로 배출됩니다.  이 혼합물은 이 조건에서 더이상 농축될 수 없으므로 두번째의 고압탑으로 보내져 분리됩니다.  두번째 탑은 고압에서 운전되며 첫번째 탑에서 분리되지 않은 혼합물을 압력이 높은 조건에서 분리합니다.  고비점 농도가 낮은 영역에서는 순수한 저비점 물질의 비점이 오히려 고비점/저비점 혼합물의 비점보다 높기 때문에 (상압에서) 저비점인 물질이 두번째 탑의 하부로 생산되고 고/저비점 혼합물은 첫번째 탑 상부로 배출된 후 첫번째 탑으로 순환되고 Fresh Feed와 합해져 증류됩니다. Pressure Swing은 하나의 탑을 이용하여 압력을 달리하며 운전하는 것을 말하는데 두개의 탑을 이용하는 것이 정상상태로 운전하는 것이라서 운전이 용이합니다. (1) Pressure-Swing-Distillation은 혼합물이 공비점을 가지고 있어서 단순증류로 분리되지 않는 경우에 적용하는 방법의 하나입니다. 압력을 달리하면 공비점이 없어지는 경우라면 단순히 압력만 달리하면 되지만 압력이 달라짐에 따라 공비점 농도가 달라지는 경우에 사용되는 방법입니다. 이곳을 먼저 찾아보도록 하세요. http://en.wikipedia.org/wiki/Azeotrope#Pressure_swing_distillation http://www.separationprocesses.com/Distillation/DT_Chp06g.htm (2) 논문이 잘못된 것이 아닙니다. 언급한 논문을 자세히 읽어보면 왜 두번째 탑하부로 비점낮은 물질이 얻어지는지 알 수 있을 것입니다. 질문의 경우, 위의 두번째 URL링크에 소개된 경우와 같은 조건에서 운전되는 것입니다. (공비혼합물이 각 물질의 비점보다 낮은 비점을 가지고 압력을 높이면 공비점이 높은 농도쪽으로 이동하는 경우에 해당합니다.) (3) 분리원리 첫번째 탑은 저압으로 운전되는데 일반 증류탑에서와 같이 고비점 물질의 비점이 혼합물의 비점보다 더 높으므로 탑의 하부로 순수한 (상압에서의) 고비점 물질이 얻어집니다. 상부로는 낮은 비점의 고비점/저비점이 혼합물 상태로 배출됩니다. 이 혼합물은 이 조건에서 더이상 농축될 수 없으므로 두번째의 고압탑으로 보내져 분리됩니다. 두번째 탑은 고압에서 운전되며 첫번째 탑에서 분리되지 않은 혼합물을 압력이 높은 조건에서 분리합니다. 고비점 농도가 낮은 영역에서는 순수한 저비점 물질의 비점이 오히려 고비점/저비점 혼합물의 비점보다 높기 때문에 (상압에서) 저비점인 물질이 두번째 탑의 하부로 생산되고 고/저비점 혼합물은 첫번째 탑 상부로 배출된 후 첫번째 탑으로 순환되고 Fresh Feed와 합해져 증류됩니다. Pressure Swing은 하나의 탑을 이용하여 압력을 달리하며 운전하는 것을 말하는데 두개의 탑을 이용하는 것이 정상상태로 운전하는 것이라서 운전이 용이합니다.

Moon mun1107a   14-06-05 20:19 와 제가 몰랐던 새로운 지식에 감탄하며 갑니다. 단지 "증류탑에서 저비점 물질은 기상으로 고비점 물질은 액상으로 간다" 같이 단순하게 생각하고 있었는데, 혼합물 일때 순수한 물질의 비점보다 낮아질 수 있음을 간과 하고 있었네요. 감사합니다. 와 제가 몰랐던 새로운 지식에 감탄하며 갑니다. 단지 "증류탑에서 저비점 물질은 기상으로 고비점 물질은 액상으로 간다" 같이 단순하게 생각하고 있었는데, 혼합물 일때 순수한 물질의 비점보다 낮아질 수 있음을 간과 하고 있었네요. 감사합니다.

스테파노 Stefano   14-06-11 10:04 (1) 압력을 달리해야 하는 이유는 공비 혼합물로 배출되는 물질은 혼합물의 비점이 같아서 더 이상 농도변화가 없기 때문입니다.  공비점혼합물에 도달하기 전에 배출한 후 압력을 달리하여 증류하는 것이지요.    (2) 압력이 다른 각 증류탑의 (상부 혹은 하부) 한쪽으로는 순성분이, 다른 쪽으로는 혼합물이 얻어지는데 이 혼합물들을 서로 분리가능한 영역으로 옮겨가기 위하여 (한개의 Tower내에서 혹은 두개의 Tower를 옮겨다니며) 압력을 높였다 낮추었다 하기 때문에 "Pressure-Swing"이라는 용어를 사용합니다.  공비증류, 추출증류에 비하여 에너지 효율이 떨어지지만 제3의 다른 물질을 사용하지 않는 분리방법입니다. (1) 압력을 달리해야 하는 이유는 공비 혼합물로 배출되는 물질은 혼합물의 비점이 같아서 더 이상 농도변화가 없기 때문입니다. 공비점혼합물에 도달하기 전에 배출한 후 압력을 달리하여 증류하는 것이지요. (2) 압력이 다른 각 증류탑의 (상부 혹은 하부) 한쪽으로는 순성분이, 다른 쪽으로는 혼합물이 얻어지는데 이 혼합물들을 서로 분리가능한 영역으로 옮겨가기 위하여 (한개의 Tower내에서 혹은 두개의 Tower를 옮겨다니며) 압력을 높였다 낮추었다 하기 때문에 "Pressure-Swing"이라는 용어를 사용합니다. 공비증류, 추출증류에 비하여 에너지 효율이 떨어지지만 제3의 다른 물질을 사용하지 않는 분리방법입니다.

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