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  Column Hot Bypass Control °ü·Ã ¹®ÀÇ
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´ÙÀ½ ³»¿ëÀº Distillation Operation (Henry Kister)¿¡ ³ª¿À´Â ³»¿ëÀÔ´Ï´Ù.
The hot vapor bypass arrangement, however, has several disadvantages, and its operation can be troublesome. Because of the liquid leg between the condenser and the drum, this technique can suffer from interaction between the drum and the condenser liquid level and from U-tube oscillations. To minimize the interaction, the pressure controller should be tuned much tighter than the drum level controller. There is an inverse response problem ; when pressure rises, it closes the bypass valve, which initially causes a further increase in pressure until the condenser level begins to fall. There is a reliance on subcooling in order to enable upward liquid movement and condensation of hot vapor against the drum surface. Operation may be troublesome if the drum liquid surface is agitated; a case of instability due to inadvertent agitation has been reported. Since the success of this technique is contingent on maintaining a small vapor pressure difference, the reflux drum vapor space needs to be insulated to minimize interference from rainstorms. The above instabilities appear to be more pronounced with narrow boiling-range mixtures, and at high pressures, where small temperature changes have a large effect on the split of overhead flow between the condenser and bypass.
 
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at high pressures, where small temperature changes have a large effect on the split of overhead flow between the condenser and bypass.
ºÎºÐÀÌ Àß ÀÌÇØ°¡ ¾È °¡³×¿ä...
 
¿Ö °í¾Ð¿¡¼­ ¿îÀüµÇ´Â °æ¿ì¿¡ ¾à°£ÀÇ ¿Âµµ Â÷ÀÌ°¡ condenser / bypassÀÇ split¿¡ ¿µÇâÀÌ Å©´Ù°í ÇÒ±î¿ä?
 
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½ºÅ×Æijë Stefano   16-09-13 09:44
<´Ü¼øÈ÷ ¾Ð·ÂÀÇ ³ô´Ù´Â ÀÌÀ¯¸¸ÀÇ ¿µÇâ>ÀÌ ¾Æ´Ï¶ó <narrow boiling-range mixtureÀε¥´Ù°¡ ¾Ð·ÂÀÌ ³ôÀ» °æ¿ì>¶ó°í ÀÌÇØÇØ¾ß ÇÕ´Ï´Ù. 

ºñÁ¡Â÷ÀÌ°¡ Å©°Ô ³ªÁö ¾Ê´Â ¹°ÁúÀÌ Top Overhead Vapor¿¡ Æ÷ÇԵǾî ÀÖÀ»°æ¿ì ¿Âµµ°¡ Á¶±Ý¶³¾îÁö¸é Heavier ¼ººÐÀÌ ÀÀÃàÇÏ°Ô µÇ¾î ¾Ð·ÂÀÌ ³·¾ÆÁüÀ¸·Î½á ¾×¸éÀÇ º¯È­¿Í ÇÔ²² Reflux DrumÀ¸·Î Èê·¯µé¾î¿Â Cold Condensate¿¡ Hot Vapor°¡ ÀÀÃàµÇ¾î Condenser ¹× Reflux Drum °¢°¢ÀÇ Liquid Level Èçµé¸²°ú µ¿¹ÝÇÏ¿© ºÒ¾ÈÁ¤ÇÑ »óÅ°¡ À¯ÁöµÇ´Âµ¥,

¾Ð·ÂÀÌ ³ôÀ» °æ¿ì Vapor Mixture¿¡ Heavier ¼ººÐÀÇ Àý´ë·®ÀÌ ´õ ¸¹¾Æ¼­ Ãæ°ÝÀÇ Å©±â°¡ ´õ Å©´Ù´Â °ÍÀÌ  µÞ¹è°æ¿¡ ±ò¸µÀ̾߱âÁö¿ä.
     
Çϳ¯ chem002233   16-09-13 13:34
½ºÅ×ÆÄ³ë ´Ô!!
Áú¹®ÀÌ¿ä.

1. ¿©±â¼­ Liquid Leg¶ó´Â ¸»Àº Á¦°¡ ÀÎÅͳݿ¡¼­ ã¾ÒÀ¾´Ï´Ù.
Liquid Leg : Reflux Condenser¿¡¼­ ÀÀÃàµÈ Condensate´Â Reflux DrumÀ¸·Î À̵¿Çϴµ¥, À̶§ Condensate°¡ Sub-cooling µÇ°í Sub-cooling µÈ Condensate°¡ Reflux Drum »óºÎ·Î µµÀԵǴ °æ¿ì Drum »óºÎ¿¡ ÀÖ´Â Vapor¸¦ ±Þ°ÝÈ÷ ÀÀÃà½ÃÅ°°Ô µÇ°í Vapor ÀÀÃàÀ¸·Î ÀÎÇÑ Impact°¡ "Liquid Leg"¶ó°í ÇÏ´õ¶ó°í¿ä.
(½ºÅ×Æijë´Ô È®ÀÎ ºÎŹ µå¸³´Ï´Ù.)

2. The Split of Overhead flow between the condenser and bypass : ÀÌ°ÍÀÌ ¹«¾ùÀ» ¸»ÇÏ´ÂÁö ¸ð¸£°Ú³×¿ä.

¿©·¯°¡Áö ¹è¿ï°Ô ¸¹Àº »ç¶÷ ÀÔ´Ï´Ù. ¸¹Àº °¡¸£Ä§ ºÎŹ µå¸³´Ï´Ù.
½ºÅ×Æijë Stefano   16-09-13 14:43
(A1) º» ÁÖÁ¦¿Í °ü·ÃµÈ Liquid Leg´Â Condenser¿Í Reflux Drum°£À» Condensate·Î ¿¬°áµÈ °üÀ» ¸»ÇÕ´Ï´Ù.  Áú¹®¿¡¼­ÀÇ °æ¿ì´Â °ú³ÃµÈ ÀÀÃà¼ö°¡ Reflux Drum Ç¥¸é¿¡ ¶³¾îÁ® Vapor°¡ Drum ¾×¸éÀ§¿¡¼­ ÀÀÃàµÇ´Â Çö»óÀ» ÁöĪÇÏ´Â °ÍÀ¸·Î º¸À̴µ¥ À̸¦ µÎ°í Liquid Leg¶ó°í Çß´Ù¸é ¿ë¾î¾²ÀÓÀÌ À߸øµÈ °ÍÀÔ´Ï´Ù. 

Condensate°¡ Condenser¿¡¼­ ÀÀÃàµÈ ÈÄ SubcoolingÀÌ ¸¹ÀÌ µÉ°Í °°Áö¸¸ ½ÇÁ¦·Î´Â ÀÀÃàµÇ¸é¼­ ÀÀÃàÀá¿­À» ³»³õ±â ¶§¹®¿¡ ½ÇÁ¦·Î SubcoolingÀÌ ¸¹ÀÌ ÀϾÁö ¾Ê°í Reflux Drum¿¡ ¿Í¼­ ÀÀÃàµÇ´Â Çö»óµµ ¾ÆÁÖ ¹Ì¹ÌÇϱ⠶§¹®¿¡ ¹«½ÃÇصµ µÇÁö¿ä.

(A2) Overhead Vapor°¡ °¥¶óÁ® Çϳª´Â Condenser·Î Çϳª´Â Reflux DrumÀ¸·Î ¿¬°áµÇ´Â °ÍÀ» "Split of Overhead Flow"¶ó°í ÇÑ °ÍÀÔ´Ï´Ù.  ÀÌÁß  ÈÄÀÚ¸¦ À§ÇØ ¿¬°áµÈ °üÀ» Hot Vapor Bypass Line  ȤÀº Condenser Bypass LineÀ̶ó°í ÇÕ´Ï´Ù.
     
Çϳ¯ chem002233   16-09-19 12:58
»ó¼¼ÇÑ ¼³¸í °¨»çµå¸³´Ï´Ù.
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